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Multicore fiber temperature sensor with fast response times

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Abstract

A multicore fiber (MCF) based temperature sensor was fabricated and packaged into a stainless-steel tube to protect the bare-fiber, and it offers a commercial friendly form factor. The sensor displayed a periodic supermode interference pattern that red-shifts with increasing temperature, which was used to calibrate the sensor. Additionally, an economical photodiode-based interrogator was fabricated from off-the-shelf parts and used to calibrate the sensor in both liquid and gas mediums. The response time to changes in temperature for the MCF sensor was found to be an order of magnitude faster than a thermocouple of identical diameter, 0.09 s compared to >1.0 s, respectively.

© 2018 Optical Society of America under the terms of the OSA Open Access Publishing Agreement

1. Introduction

Fiber optic sensors (FOS) offers many advantages over conventional sensors, such as corrosion resistance, multiplexing, compact design, and immunity from many types of electromagnetic radiations [1–4]. Because of these advantages, FOS is a very active research field covering a host of applications: biomedical applications, vibrational detection, bridge monitoring, and temperature sensing [4–8]. In the case of temperature sensing, many types of FOS have been investigated; however, most of these sensors suffer from some limitations.

Fiber Bragg grating (FBG) sensors are a popular commercially available FOS. FBGs are compact, reliable, and easy to integrate into existing systems. However, FBG require expensive interrogation equipment and standard Type I gratings have a maximum temperature of only a few hundred degrees Celsius [9,10], limiting the possible applications that FBG can be used for. For higher temperatures, photonic crystal fibers (PCF) have received considerable attention for their ability to operate stably up to 1100 °C [11,12]. These high temperature sensors are created by splicing a section of PCF between standard single mode fiber (SMF), resulting in a Fabry-Perot type interferometer [13,14]. However, these types of PCF interferometers require complex fabrication including offset splicing and collapsing of sections of the PCF splice [11,13]. Recently, multicore fiber (MCF) based FOS have been fabricated that are thermally-stable at high temperature (1000 °C), cost efficient, and easy to fabricate; offering an attractive alternative to FGB and PCF [15–17].

Amezcua-Correa et al. [15–17] demonstrated that a section of MCF spliced between two SMF sections, similar to the PCF-type sensors, can be used to accurately measure temperature. The MCF is comprised of seven cores arranged in a symmetric hexagonal shape, Fig. 1

 figure: Fig. 1

Fig. 1 Seven Core MCF (a) schematic of MCF with hexagonal core shape, (b) microscope image of MCF, (c) microscope image with small reflection on bottom right that clearly shows the geometry of the MCF, and (d) periodic interference pattern of SMF-MCF-SMF device.

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. Typically, seven coupled cores would produce seven possible supermodes; however, the fundamental mode of the SMF can only excite two of the seven MCF supermodes. The two excitable modes interfere in the MCF section to produce a periodic interference pattern, Fig. 1 shows an interference pattern producing two peaks. The periodicity of the interference pattern is dependent on the length of the MCF section, with longer sections of MCF decreasing the periodicity (increasing the number of interference peaks) [15]. In addition to the length of the MCF section, the interference pattern is also dependent on the temperature of the fiber. Changes in temperature change both the refractive index of the fiber and causes physical deformation (expansion and contraction). With increasing temperature, the interference peaks shift to higher wavelengths. Previous studies demonstrated a linear relationship between temperature and peak wavelength, and this relationship is used to calibrate SMF-MCF-SMF devices [15].

The purpose of this study was to produce a commercially viable MCF temperature sensor operating in reflection mode. An MCF sensor was packaged into a 0.559 mm diameter stainless steel tube, Fig. 2

 figure: Fig. 2

Fig. 2 Experimental setup consists of a light source, fiber optical circulator, packaged MCF temperature sensor, and spectrometer or optical interrogator (depending on experiment). MCF temperature sensor consists of a 5mm section of MCF fusion spliced between two SMFs. The Sensor is packaged into a stainless tube and operated in reflection mode.

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. The MCF sensor was calibrated using two different optical interrogation devices. The first method of calibration used a spectrometer, and the calibration was performed based on wavelength shift. The second calibration method used a photodiode and calibrated based on the output current. Additionally, it was determined that the response time of the MCF temperature sensor is an order of magnitude faster than a thermocouple (TC) of identical dimensions. Although a similar MCF-based strain sensor [8], has been packaged and operated in reflection mode, we believe this is the first study to report on an MCF packaged temperature sensor; all previous reports used bare-fiber sensors. Furthermore, this is the first study to report on the use of an inexpensive photodiode-based interrogator to calibrate an MCF temperature sensor.

2. Sensor fabrication

The MCF temperature sensor was fabricated by fusion splicing a 5 mm section of MCF between two sections of SMF, Fig. 2. The MCF was 3rd generation MCF, purchased from The College of Optics and Photonics (CREOL) at University of Central Florida. To operate in reflective mode, the end of one of the SMFs was coated with a reflective metal. The fiber was then packaged into a stainless tube of 0.559 mm diameter. The stainless-steel tubing serves two purposes; it protects the bare-fiber from physical damage and it provides a support, preventing the fiber from moving. Preventing movement of the fiber is important because the same SMF-MCF-SMF sensor can also be used to measure force, strain, and curvature [16,18,19]. The stainless-steel tube prevents the fiber from moving and causing non-temperature related changes in the interference spectra. The bare fiber was not constrained to the inside of the tube, there is a slight clearance between the tube and fiber. Previous efforts to pot the fiber using ceramic cements resulted in noisy, non-usable data. We believe this is because of mis-matching thermal expansion between the fiber and cement causing stain and/or bending on the sensor. The non-coated SMF is terminated to a standard FC connector, Fig. 2.

3. Temperature detection

3.1 Spectrometer calibration

To determine the quality of the packaged MCF temperature sensor, the temperature response to the multimode interference was investigated. The experimental setup is shown in Fig. 2. The sensor was connected to a stabilized tungsten IR light source (Thorlabs, SLS202L), a fiber optic circulator, and a spectrometer (Ocean Optics, NIRQuest512-2.2). The sensor was placed into a stream of heated air of varying temperature, and the change to the spectra was observed. Figure 3(a)

 figure: Fig. 3

Fig. 3 (A) Spectral shift of MCF. With increasing temperature, the wavelength of maximum reflection shifts to larger wavelengths. (B) Linear plot shows a spectral shift 35 pm/°C.

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shows the results for three different temperatures. As expected, the interference peaks shift to higher wavelengths with increasing temperatures. Furthermore, the shift was determined to be linear with a slope of 35 pm/°C, Fig. 3(b). These results are consistent with previous studies [15]. The linear nature of the data indicates that the stainless-steel tube performed well in physically stabilizing the fiber and preventing it from bending or vibrating. These results are consistent with previous studies [15].

3.2 Photodiode calibration

Although the spectrometer worked well in demonstrating the spectral response to temperature changes in the MCF, a cheaper alternative is required if MCF sensors are to be widely distributed commercially. To this end, a low-cost optical integrator was fabricated from commercially available off-the-shelf parts, with a photodiode used as a detector. The photodiode converts light into an electrical current, and the current can be used to calibrate the packaged MCF sensor. To test the effectiveness of the photodiode-based interrogator, the packaged MCF sensor was testing in both a liquid and gas medium.

Experiments involving the photodiode-based interrogator used a monochromatic light source of 1525 nm, produce from a Golight Tunable Light Source (Shenzhen Golight Technology Co.). A mass-produced interrogator can be little more than a fiber coupled telecom laser. The choice of wavelength is not arbitrary and should be chosen to fall between a peak or valley of the interference spectrum. This is because the calibration is based on the photodiode, which outputs a value that is proportional to the reflection value, i.e. the larger the reflection percent, the larger the output of the photodiode. If the wavelength of the light source is chosen such that it falls on a peak, the reflection value will decrease with both heating and cooling. Conversely, if the wavelength of the light source is chosen such that it falls on a valley, the reflection value will increase with both heating and cooling. For example, at 200 °C the interference pattern has a λmax of 1486 nm. If 1485 nm is chosen as the wavelength of the light source, heating would cause the peak to shift 35 pm/°C [which is the slope in Fig. 3(b)] to the right, and cooling would cause the peak to shift 35 pm/°C left. A temperature of 225 °C (200 + 25) would give the same reflection value as 175 °C (200 - 25). And identical reflection values would give identical outputs from the photodiode detector. For this reason, the wavelength of the light source must be a reasonable distance from a peak or valley value in the interference spectrum.

The photodiode-based interrogator was tested by heating and cooling the MCF temperature sensor in a gas and liquid media, a hot air steam and wave oil, respectively. Figure 4

 figure: Fig. 4

Fig. 4 Temperature response of MCF temperature sensor using photodiode interrogator in a stream of heated air. (A) Counts from photodiode output on right axis, temperature (°C) on left axis. (B) The oscillations in the counts (right axis) is a product of the oscillation of the power supplied to the heating element. The PID loop of the heating element is constantly changing power (left axis), and the MCF response time is fast enough to detect these slight changes in temperature.

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shows the resulting photodiode output for a stream of heated air being passed over the sensor. The temperature was allowed to reach equilibrium and then held steady for several minutes. The temperature on the left axis is measured from a k-type thermocouple. The output of the photodiode, listed as “counts”, is displayed on the right axis. The output of the photodiode was shown to have a linear relationship with temperature in both liquid and gas mediums, which was used to calibrate the MCF temperature sensor, see Fig. 5
 figure: Fig. 5

Fig. 5 (A) MCF temperature calibration using photodiode interrogator in a gas (▲) and liquid (■) environment. (B) Error analysis demonstrated the calibration was within 5% error for all points. The line is not fit to data, it is the y = x line, and used for visual aid of calibration precision. The closer a data point is to the line, the more precise the calibration.

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. The data points in Fig. 5(a) represent the average of the counts in three-minute intervals. The average was used because of the oscillate of the photodiode output displayed in Fig. 4. The oscillations in counts is from the rapid change in temperature of the heated air. The heater is a closed looped consisting of a thermocouple, heating element and power source. Because the response time of the MCF sensor is much faster (explained below) than the TC, the MCF can detect the oscillations in the power source, Fig. 4(b).

Additionally, the error was shown to be <5% of the value for all points. Figure 5(b) shows the predicted temperatures plotted against the actual temperatures with a y = x line. The y = x line represents a calibration with zero error, the farther a data point is from the line, the greater the error. This demonstrates the practicality of using an inexpensive photodiode-based interrogator with an inexpensive MCF temperature sensor.

The differences in the calibration equations are because the sensor was calibrated at different reference temperatures on different days. Many photodiode characteristics, including the output current, are temperature dependent. The temperature in our lab is not constant, and the calibrations in Fig. 5 were performed on different days. These difference in temperatures account for the differences in calibration equations for the liquid and gas experiments. Future work involves software integration that accounts for reference temperature of the photodiode interrogator; analogous to the cold junction temperature adjustments of thermocouples [20].

One important metric in temperature sensing is response time. A common measurement to compare response times between sensors is the Time Constant (τ63%), which is the time required to reach 63.2% of an instantaneous change in temperature. Figure 6

 figure: Fig. 6

Fig. 6 Response time of the packaged MCF temperature sensor and the theoretical response time of a k-type thermocouple of identical dimensions. The MCF sensor has a τ63% of 0.09 seconds, while the TC has a theoretical τ63% > 1.0 seconds. The TC time constant was calculated from correlation charts provided by Omega [21]. The line for the TC is not meant to represent a liner relationship, the data is a starting value and a final value. The line was added for visual aid only. The TC time constant was calculated from correlation charts provided by Omega [21]. The line for the TC is not meant to represent a liner relationship, the data is a starting value and a final value. The line was added for visual aid only.

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shows the response time for the packaged MCF sensor compared to the theoretical response of a TC. The MCF sensor was held at room temperature and then plunged into a bath of 175 °C wave oil. The MCF has a τ63% of 0.09 seconds, compared to a τ63% > 1.0 seconds for a k-type TC of identical diameter. The TC response time was calculated from Omega values for a “bare wire” TC [21]. The MCF fiber, which has the stainless-steel sheath, out performs the un-sheathed bare wire TC of identical diameter. The MCF sensor has a response of 1050 °C/sec during the τ63% interval, while the TC had a response slower than 95 °C/sec. These results have promising implications for industries that require fast response time in high temperature environments, such as silicon wafer production in the semiconductor industry. The TC line in Fig. 6 is not meant to indicate a linear response, the τ63% data is two points (staring and final value) and line was added for visual aid only [21].

4. Conclusion

In conclusion, an MCF-based temperature sensor was fabricated by splicing a 5 mm section of MCF between two sections of SMF. The resulting fiber was then packaged in a 0.559 mm diameter stainless steel tube, which provides a commercial friendly formfactor. The MCF interference pattern was shown to have a linear 35 pm/°C shift to changes in temperature. The package MCF sensor was also tested and calibrated using a photodiode-based interrogator in both liquid and gas mediums, which also showed a linear temperature response. The response time was measured and compared to the theoretical response time of a TC of identical diameter. It was found that the MCF temperature sensor has a time constant of 0.09 seconds, compared to over 1.0 second for a thermocouple. To the best of our knowledge, this is the first time that a packaged MCF temperature device has been reported, all other reports used an exposed bare-fiber sensor. Additionally, this is the first known reporting which used a photodiode-based interrogator to measure the response from the MCF sensor. The combination of these two firsts, demonstrates the feasibility of an inexpensive and highly responsive fiber optic-based temperature sensor. Future work includes creating a reference temperature adjustment for the photodiode, and a complete determination of important characteristics: resolution, sensitivity, and full temperature range.

Funding

National Science Foundation (1660213, IPP-1552305).

Acknowledgments

This material is based upon work supported by the National Science Foundation under Grant No. 1660213, by the National Science Foundation under Grant # IIP-1552305 to the American Society for Engineering Education, and by Multicore Photonics, Inc. and the Florida Institute for the Commercialization of Public Research.

References

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16. A. Van Newkirk, J. E. Antonio-Lopez, G. Salceda-Delgado, M. U. Piracha, R. Amezcua-Correa, and A. Schülzgen, “Multicore fiber sensors for simultaneous measurement of force and temperature,” IEEE Photonics Technol. Lett. 27(14), 1523–1526 (2015). [CrossRef]  

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Figures (6)

Fig. 1
Fig. 1 Seven Core MCF (a) schematic of MCF with hexagonal core shape, (b) microscope image of MCF, (c) microscope image with small reflection on bottom right that clearly shows the geometry of the MCF, and (d) periodic interference pattern of SMF-MCF-SMF device.
Fig. 2
Fig. 2 Experimental setup consists of a light source, fiber optical circulator, packaged MCF temperature sensor, and spectrometer or optical interrogator (depending on experiment). MCF temperature sensor consists of a 5mm section of MCF fusion spliced between two SMFs. The Sensor is packaged into a stainless tube and operated in reflection mode.
Fig. 3
Fig. 3 (A) Spectral shift of MCF. With increasing temperature, the wavelength of maximum reflection shifts to larger wavelengths. (B) Linear plot shows a spectral shift 35 pm/°C.
Fig. 4
Fig. 4 Temperature response of MCF temperature sensor using photodiode interrogator in a stream of heated air. (A) Counts from photodiode output on right axis, temperature (°C) on left axis. (B) The oscillations in the counts (right axis) is a product of the oscillation of the power supplied to the heating element. The PID loop of the heating element is constantly changing power (left axis), and the MCF response time is fast enough to detect these slight changes in temperature.
Fig. 5
Fig. 5 (A) MCF temperature calibration using photodiode interrogator in a gas (▲) and liquid (■) environment. (B) Error analysis demonstrated the calibration was within 5% error for all points. The line is not fit to data, it is the y = x line, and used for visual aid of calibration precision. The closer a data point is to the line, the more precise the calibration.
Fig. 6
Fig. 6 Response time of the packaged MCF temperature sensor and the theoretical response time of a k-type thermocouple of identical dimensions. The MCF sensor has a τ63% of 0.09 seconds, while the TC has a theoretical τ63% > 1.0 seconds. The TC time constant was calculated from correlation charts provided by Omega [21]. The line for the TC is not meant to represent a liner relationship, the data is a starting value and a final value. The line was added for visual aid only. The TC time constant was calculated from correlation charts provided by Omega [21]. The line for the TC is not meant to represent a liner relationship, the data is a starting value and a final value. The line was added for visual aid only.
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