I | Fluorescence begins | 19900 | | |
| Strong, broad | 19740 | 19766 | Moderate, broad |
| Moderate, diffuse | 19530 | 19542 | Weak, diffuse |
| Moderate, very diffuse | 19150 | 19245 | Weak, very diffuse |
II | Strong, diffuse | 18920 | 18937 | Strong, broad |
| Weak, very diffuse | 18740 | 18706 | Weak, diffuse |
| Weak, very diffuse | 18410 | 18472 | Weak, very diffuse |
III | Moderate, diffuse | 18080 | 18090 | Moderate, broad |
IV | Weak, very diffuse | 17420 | present | Weak, very diffuse |
|
First band at 19,740 cm−1. Bands repeat every 833±9 cm−1. Secondary lines in bands at 200 cm−1 and 550 cm−1 from initial line. (Note: the average deviation given after frequency with which bands repeat is probably much less than the actual error in this and all other tables.) | The bands are fairly sharp with structure. Total intensity is low. First band at 19,766 cm−1; bands repeat every 838±9 cm−1. Secondary lines in bands at 230 cm−1 and 500 cm−1 from initial line. |
|
B: UO3·2H2O, X-ray type IIA; Sample 235.39.2. |
|
I | Fluorescence begins | 19900 | | |
| Moderate, very diffuse; shaded to red | 19720 | 19540 | Weak, very diffuse |
II | Strong, very diffuse | 18920 | 18820 | Moderate, very diffuse; shaded to red |
III | Moderate, very diffuse | 18110 | 17961 | Weak, very diffuse; shaded to red |
IV | Extremely weak, very diffuse | present | present | Very weak, very diffuse |
|
Bands similar to x-ray type I except for absence of secondary structure. First band at 19720 cm−1 Bands repeat every 805±5 cm−1. | Bands very diffuse. Total intensity high. First band at 19540 cm−1. Bands repeat every 790±70 cm−1. |
|
C: UO3·H2O, X-ray type IIA; Sample 219.108.1. |
|
I | Fluorescence begins | 19990 | | |
| Moderate, very diffuse; shaded to red | 19730 | 19549 | Weak, very diffuse |
II | Strong, very diffuse | 18860 | 18640 | Moderate, very diffuse; shaded to red |
III | Moderate, very diffuse | 18050 | 17888 | Weak, very diffuse; shaded to red |
IV | | | present | |
|
Spectrum almost identical with that of UO3·2H2O, x-ray type IIA. First band at 19730 cm−1. Bands repeat every 835±25 cm−1. | Spectrum almost identical with that of UO3·2H2O, x-ray type IIA. Bands very diffuse. Total intensity moderate. First band at 19549 cm−1. Bands repeat every 831±79 cm−1. |
|
D: UO3·H2O, X-ray type IIB; Sample 219.92.3. |
|
I | Fluorescence begins | 19875 | | |
| Moderate, sharp | 19846.7 | 19866 | Moderate |
| Weak, narrow | 19821.3 | | |
| Weak, narrow (also center of broad band) | 19773 | 19791 | Weak |
| Weak, narrow | 19570.2 | 19584. | Weak, broad |
| Weak, narrow | 19549.3 | | |
| Moderate, broad | 19446 | 19470 | Weak, broad |
| Moderate, broad | 19420 | | |
| Moderate, broad | 19274 | 19300 | Weak, diffuse |
| Moderate, broad | 19181 | present | Very weak |
| Weak, narrow | 19030.5 | | |
II | Strong, narrow | 18998.9 | 18997 | Strong, broad |
| Very weak, narrow | 18974 | | |
| Strong, diffuse | 18909 | 18919 | Strong |
| Strong, diffuse | 18732 | 18745 | Weak, diffuse |
| Strong, diffuse | 18631 | 18605 | Weak, diffuse |
III | Strong, diffuse | 18140 | 18190 | Moderate, broad |
| Strong, diffuse | 18050 | 18067 | Moderate, broad |
| Very weak, very diffuse | 17870 | 17918 | Weak, diffuse |
| Weak, diffuse | 17800 | 17817 | Weak, diffuse |
IV | Weak, very diffuse | 17330 | 17349 | Weak, very diffuse |
| Moderate, very diffuse | 17180 | | |
V | | | present | Extremely weak, very diffuse |
|
First band at 19846.7 cm−1. Bands repeat every 839±19 cm”1. Secondary lines in bands at 25 cm−1, 90 cm−1, 270 cm−1, and 380 cm−1 from initial line. | Bands fairly sharp, with structure. Total intensity moderate. First band at 19866 cm−1. Bands repeat every 839±21 cm−1. Secondary lines in bands at 80 cm−1, 270 cm−1, and 380 cm−1 from initial line. |
|
E: UO3·H2O, X-ray type IIC; Sample 219.46.2. |
|
I | Fluorescence begins | 19797 | | |
| Moderate, sharp | 19744.5 | 19832 | Very weak |
| Strong, sharp | 19711.6 | | |
| Moderate, narrow | 19676.8 | | |
| Moderate, narrow | 19640.0 | 19635 | Moderate, very diffuse |
| Moderate, narrow | 19503.8 | | |
| Moderate, sharp | 19467.0 | | |
| Moderate | 19152 | present | Very weak |
II | Moderate | 19009.7 | 19004 | Weak, broad |
| Strong, narrow | 18991.6 | | |
| Strong | 18946.6 | | |
| Strong, very diffuse | 18896.2 | 18840 | Strong, very diffuse |
III | Strong, very diffuse | 18080 | 18157 | Weak, diffuse |
| Strong, very diffuse | 17980 | 17976 | Moderate, very diffuse |
IV | Moderate, very diffuse | (17240) | 17085 | Weak, very diffuse |
V | | | present | Very weak, very diffuse |
|
First band at 19744.5 cm−1. Band structure does not appear to repeat. Bands repeat at 835±20 cm−1. | Bands diffuse. Total intensity high. First band at 19832 cm−1. Bands repeat at 849±15 cm−1. |
|
F: UO3·H2O, X-ray type III; Sample 235.38. |
|
I | Fluorescence begins | 20030 | | |
| Very weak, narrow | 19988.6 | | |
| Weak, narrow | 19962.9 | | |
| Weak, narrow | 19938.2 | | |
| Moderate, narrow | 19876.8 | | |
| Moderate | 19825.9 | | |
| Moderate, narrow | 19773.0 | | |
| Weak | 19740.2 | | |
| Weak | 19711.0 | | |
| Strong, very diffuse | 19640 | 19681 | Weak, very diffuse |
| Moderate, very diffuse | 19120 | 19009 | Very weak, very diffuse |
II | Strong, very diffuse | 18860 | 18833 | Strong, very diffuse |
III | Strong, very diffuse | 18110 | 17993 | Weak, very diffuse |
IV | Moderate, very diffuse | 17360 | present | Very weak, very diffuse |
|
First band at 19988.6 cm−1. Bands repeat (but not the structure) every 760±13 cm−1. | Bands diffuse. Total intensity low. First band at 19681 cm−1. Bands repeat every 844±4 cm−1 |
|
G:
, X-ray type IV; Sample 235.26. |
|
I | Strong, very sharp | 19711.9 | | |
| Weak, narrow | 19009.4 | | |
| Weak, narrow | 18992.1 | | |
| Moderate, sharp | 18946.8 | | Absent |
| Moderate, sharp | 18913.4 | | |
| Strong | 18845 | | |
II | Strong, broad | 18764.2 | (18780) | Fluorescence begins, very diffuse |
| Moderate, sharp | 18755.4 | | |
| Moderate, narrow | 18672.5 | | |
| Moderate, narrow | 18656.1 | | |
| Strong, narrow | 18463.1 | (18600) | Weak, narrow |
III | Moderate, broad | 18048.7 | (18190) | Weak, narrow |
| Moderate, broad | 18023.8 | | |
| Strong, narrow | 17967.3 | (18070) | Weak, narrow |
| Strong, narrow | 17910.3 | | |
| Weak, broad | 17883.8 | | |
| Moderate, broad | 17760 | (17920) | Very weak, broad |
| Moderate, broad | 17630 | (17820) | Very weak, broad |
IV | Moderate, very diffuse | (17180) | (17180) | Very weak, very diffuse |
|
Total intensity high. First band at 19711.9 cm−1. Band structure does not appear to repeat, nor are the intervals between band peaks equal. | Fluorescence, but too weak to measure accurately. Very diffuse bands also present. First band begins at 18780 cm−1. Spectrum very much like x-ray type IIB, but first two strong bands are missing. |